SINTESIS SILIKA GEL TERIMOBILISASI DIFENILKARBAZON DARI ABU SEKAM PADI MELALUI TEKNIK SOL GEL

  • Ni Nyoman Sri Nopianingsih
  • I Wayan Sudiarta
  • Wahyu Dwijani Sulihingtyas

Abstract

A research on synthesis diphenylcarbazone immobilized silica gel from rice husk ash by sol-gel technique has been conducted. The purpose of this research was to synthesize the diphenylcarbazone immobilized silica gel from rice husk ash by sol-gel technique.  This research included modification of silica gel of rice husk ash and silica gel characterization by IR spectra and X-RD.

The results showed that the diphenylcarbazone immobilized silica gel has been successfully synthesized. It can be seen from the FTIR spectrum that silica-imobilized revealed peaks at wave numbers of ±1087.85cm-1 indicating the presence of Si-O-Si. The peak seen at wave numbers of  ±952.84cm-1 indicating the presence of Si-O, at ±3361.93cm-1due to the Si-OH bond which was the main functional group  of silica gel. Another peaks at ±3313.71cm-1, ±800.46cm-1, ±1602.85cm-1,±1700 cm-1, and ±1602.85cm-1 suggesting the presence of N-H, aromatic C-H (substituted benzene), aromatic C=C, N=N and C=O stretching. X-RD data showed that the structure of diphenilcarbazone immobilized silica gel was amorphous.

Downloads

Download data is not yet available.

Author Biographies

Ni Nyoman Sri Nopianingsih

Jurusan Kimia FMIPA Universitas Udayana, Kampus Bukit Jimbaran, Bali

I Wayan Sudiarta
Jurusan Kimia FMIPA Universitas Udayana, Kampus Bukit Jimbaran, Bali
Wahyu Dwijani Sulihingtyas
Jurusan Kimia FMIPA Universitas Udayana, Kampus Bukit Jimbaran, Bali
Published
2015-07-01
How to Cite
NOPIANINGSIH, Ni Nyoman Sri; SUDIARTA, I Wayan; SULIHINGTYAS, Wahyu Dwijani. SINTESIS SILIKA GEL TERIMOBILISASI DIFENILKARBAZON DARI ABU SEKAM PADI MELALUI TEKNIK SOL GEL. Jurnal Kimia (Journal of Chemistry), [S.l.], july 2015. ISSN 2599-2740. Available at: <https://ojs.unud.ac.id/index.php/jchem/article/view/16339>. Date accessed: 21 nov. 2024. doi: https://doi.org/10.24843/JCHEM.2015.v09.i02.p13.
Section
Articles

Keywords

rice ash, silica gel, diphenylcarbazone

Most read articles by the same author(s)

1 2 > >>