STUDI REAKSI SIKLOPENTILSILAN DENGAN 4-IODIDA THIOANISOL MENGGUNAKAN KATALIS PALADIUM

  • Aldes Lesbani
  • Risfidian Mohadi
  • Elfita Elfita

Abstract

A study on cyclopentylsilane reaction in tetrahydrofuran with 4-iodo thioanisol has been carried out using palladium as catalyst under argon atmosphere at room temperature.

The results showed that the product was tris(4-thioanisyl)cyclopentylsilane (1) which was obtained from recrystallization using methanol with the yield 35%. The Compound (1) has a melting point of 91.5-92.0 oC. Analysis using GC-MS found m/z 466 with six equivalent protons and eight carbons peak obtained from 1H and 13C NMR.

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Author Biographies

Aldes Lesbani

Staf Pengajar Jurusan Kimia FMIPA Universitas Sriwijaya

Kampus Inderalaya Km.32 Ogan Ilir Sumatera Selatan 30662

Risfidian Mohadi

Staf Pengajar Jurusan Kimia FMIPA Universitas Sriwijaya

Kampus Inderalaya Km.32 Ogan Ilir Sumatera Selatan 30662

Elfita Elfita

Staf Pengajar Jurusan Kimia FMIPA Universitas Sriwijaya

Kampus Inderalaya Km.32 Ogan Ilir Sumatera Selatan 30662

Published
2013-07-01
How to Cite
LESBANI, Aldes; MOHADI, Risfidian; ELFITA, Elfita. STUDI REAKSI SIKLOPENTILSILAN DENGAN 4-IODIDA THIOANISOL MENGGUNAKAN KATALIS PALADIUM. Jurnal Kimia (Journal of Chemistry), [S.l.], july 2013. ISSN 2599-2740. Available at: <https://ojs.unud.ac.id/index.php/jchem/article/view/8219>. Date accessed: 06 june 2020. doi: https://doi.org/10.24843/JCHEM.2013.v07.i02.p01.
Section
Articles

Keywords

cyclopentylsilane, 4-iodo thioanisol, palladium

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