Analisis Fase Karbon Pada Pemutih Gigi Berbasis Arang Aktif Tempurung Kelapa Dengan Metode Difraksi Sinar-X (XRD)
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https://doi.org/10.24843/BF.2024.V25.i01.p16
Abstrak
Sekarang telah banyak beredar di pasaran produk pemutih gigi yang diklaim terbuat dari arang tempurung kelapa. Arang di dalam suatu material adalah dalam bentuk senyawa karbon, dapat dalam bentuk fase grafit (GP), Grafen Oksida (GO), dan/atau grafen oksida tereduksi (rGO). Salah satu metode untuk mengidentifikasi keberadaan fase karbon tersebut adalah dengan menggunakan metode X-Ray Diffraction (XRD). Pada penelitian ini dilakukan karakterisasi XRD terhadap salah satu pemutih gigi berbahan dasar arang tempurung kelapa yang telah terdaftar di BPOM. Analisis fase karbon dilakukan dengan menggunakan softwae Match-3 dan Origin 2019a. Hasil analisis menunjukkan bahwa sampel pemutih gigi mengandung karbon dalam fase kristal grafit turbostratik dan amorf grafen oksida tereduksi dengan persentase kandungan masing masing adalah 1,48% dan 81,69%. Hasil analisis juga menunjukkan adanya senyawa logam P, Al, dan Si.
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Referensi
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[2] Frischa M. Wachid, Adhi Y. Perkasa, Darminto, Synthesis and Characterization of Nanocrystalline Graphite from Coconut Shell with Heating Process, AIP Conference Proceedings 1586, 2014, pp. 202–206.
[3] Siburian, R., Sari, D. R., Gultom, J., Sihotang, H.. Raja, S. L. and Supeno, M., Performance of graphite and graphene as electrodes in primary cell battery, Journal of Physics: Conf. Series, 1116, 2018, pp. 042034.
[4] Fatima Tuz Johra, Jee-Wook Lee, Woo-Gwang Jung, Facile and safe graphene preparation on solution based platform, Journal of Industrial and Engineering Chemistry, Vol. 20, 2014, pp. 2883-2887.
[5] ISO/TS 80004-11:2017 (en), Nanotechnologies-Vocabulary-Part 11: Nanolayer, Nanocoating, Nanofilm and related terms, Technical Committee ISO/TC 229, Nanotechnologies, 2017.
[6] Krzysztof Tadyszak, Jacek K. Wychowaniec, and Jagoda Litowczenko Biomedical Applications of Graphene-Based Structures, Nanomaterials, Vol. 8, 2018, pp. 944.
[7] Franziska Schäffel, The Atomic Structure of Graphene and Its Few-layer Counterparts, In: Jamie H. Warner, Franziska Schäffel, Alicja Bachmatiuk, Mark H. Rümmeli, Graphene: Fundamentals and Emergent Applications, Elsevier Inc, 2013.
[8] Michio Inagaki, Advanced Carbon Materials, In: Shigeyuki Somiya, Second Edition, Handbook of Advanced Ceramics: Materials, Applications, Processing, and Properties, Elsevier Inc., 2013.
[9] Michael C. Rowe, Brendon J. Brewer, AMORPH: A statistical program for characterizing amorphous materials by X-ray diffraction, Computers & Geosciences, Vol. 120, 2018, pp. 21-31.
[10] Atom Hamasaki, Ayumi Furuse, Yuya Sekinuma, Kazuki Fujio, Masashi Iide & Sumio Ozeki, Improving the Micropore Capacity of Activated Carbon by preparation under a High Magnetic Field of 10 T, Scientific Reports, Vol. 9, 2019, pp. 7489.
[11] Rifki Husnul, K, Pembuatan dan Karakterisasi Karbon Aktif dari Tempurung Kelapa Sebagai Adsorsben Zat Warna Metilan Biru, Universitas Lampung, 2016.
[12] Garg A., Textbook of Operative Dentistry. 3rd ed., New Delhi, Jaypee, 2015, pp. 443-462.
[13] Annisa Athirah, Pengaruh Waktu Aktivasi Arang Tempurung Kelapa (Cocos Nucifera) Sebagai Alternatif Bahan Home Bleaching Alami Terhadap Perubahan Kecerahan Gigi (In Vitro), Skripsi, Fakultas Kedokteran Gigi Universitas Sumatera Utara Medan, 2019.
[14] Pambayun, G. S., Yuliantom, R.Y.E., Rachimoellah M., Putri E.M.M, Pembuatan karbon aktif dari arang tempurung kelapa dengan aktivator ZnCl2 dan Na2CO3 sebagai adsorben untuk mengurangi kadar fenol dalam air limbah”. Jurnal Teknik POMITS, Vol. 2(1), 2013, pp. 116–120.
[15] Fatima Tuz Johra, Jee-Wook Lee, Woo-Gwang Jung, Facile And Safe Graphene Preparation on Solution Based Platform, Journal of Industrial and Engineering Chemistry, Vol. 20, 2014, pp. 2883-2887.
[16] Sujiono, E.H., Zurnansyah, D. Zabrian, M.Y. Dahlan, B.D. Amin, Samnur, J. Agus, Graphene oxide based coconut shell waste: synthesis by modified Hummers method and characterization, Heliyon, Vol.6, 2020, pp. e04568.
[17] Xinfeng Xie, Production And Characterization Of Carbon Structures Derived From Wood, Thesis, Presented in Partial Fulfillment of the Requirements for the Degree of Doctor, 2008.
[18] Fahmi, Nur Anggita Ayu Dewayanti, Widiyastuti Widiyastuti & Heru Setyawan, Preparation of porous graphene-like material from coconut shell charcoals for supercapacitors, Cogent Engineering, Vol. 7, 2008, pp. 1748962.
[19] Manoj B, Kunjomana, A.G., Study of Stacking Structure of Amorphous Carbon by X-Ray Diffraction Technique, Int., J. Electrochem. Sci., Vol. 7, 2012, pp. 3127-3134.
[20] Manoj B, Investigation of nanocrystalline structure in selected carbonaceous materials, International Journal of Minerals, Metallurgy and Materials, Vol. 21, No. 9, 2014, pp. 940-946.
Diterbitkan
2024-02-28
##submission.howToCite##
ALFIRA, Muna et al.
Analisis Fase Karbon Pada Pemutih Gigi Berbasis Arang Aktif Tempurung Kelapa Dengan Metode Difraksi Sinar-X (XRD).
BULETIN FISIKA, [S.l.], v. 25, n. 1, p. 124 – 129, feb. 2024.
ISSN 2580-9733.
Tersedia pada: <https://ojs.unud.ac.id/index.php/buletinfisika/article/view/100553>. Tanggal Akses: 04 nov. 2025
doi: https://doi.org/10.24843/BF.2024.V25.i01.p16.
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